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Pyroprobe 5000, 5150 & 5200
The CDS Pyroprobe® Model 5000 is the most advanced thermal sample preparation instrument available. Platinum filaments are rapidly heated for pulse pyrolysis work, or slowly heated with controlled rates for programmed analyses. Set temperatures in 1°C increments to 1400°C for a wide heating range and more precise pyrolysis temperatures. Analytical runs may be programmed for up to eight steps per sample, with automatic control of the on-line valve, interface temperature, GC ready sensing and GC start for each step. When configured with the trapping option, the Pyroprobe® may be used to collect analytes from slow rate pyrolysis, thermal desorption or reactant gas pyrolysis. The unique interfacing design permits a direct pyrolysis path to the GC inlet or rapid sample heating and transfer to the trap without interrupting the pneumatics of the GC. Simple PC control of all parameters is presented in an easy to program window, permitting method development, storage, notation and editing.
New! For Model 5150 and 5200 Pyroprobes:
Cryofocusing Option - produces sharper peaks for early eluting compounds.
An injection port mounted device cooled by N2 or CO2.
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| Overall Dimensions: 23 cm W x 24 cm H x 31 cm D (5000 without interface) |
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Model 5000
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Pulse Pyrolysis
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Filament Temperature
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Programmable in 1°C increments to 1400°C
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Heating Rates
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0.01 to 20.0°C/ms (10 to 20,000°C/second)
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Clean and Dry
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User selectable
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Programmed Pyrolysis
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Heating Rates
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0.01 to 999.9°C/sec and 0.01 to 999.9°C/min
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Multiple Steps
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Each step may include GC start
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1500 Valved Interface
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Isothermal temperature, set in 1°C increments
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Model 5150 - all above plus..
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Multiple steps
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Each interface step includes initial, ramp and final. Each step may include Pyroprobe® and GC start
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Interface
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Low-mass programmable zone on 5150 unit
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Temperature
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Settable in 1°C/min increments to 350°C
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Heating Rates
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Programmable in 1°C/min increments to 60°C/min
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Heated Zones
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4 auxiliary zones
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Valve Oven
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Settable in 1°C increments to 300°C
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| Transfer Line |
Settable in 1°C increments to 325°C
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Model 5200
For headspace trapping & reactant gas pyrolysis |
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Interface
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Pyrolysis to built-in trap or direct to GC
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Temperature
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Settable in 1°C increments to 350°C
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Heating Rates
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Programmable in 1°C/min increments to 60°C/min
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Trapping Tube
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Ambient to 350°C
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The test-tube desorber replaces the regular interface zone so that the top of the 5200 looks like this:
To view available accessories for Pyroprobe 1000, Pyroprobe 2000, and Pyroprobe 5000 click here
To view spare parts and consumables for Pyroprobe 1000, Pyroprobe 2000, and Pyroprobe 5000 click here.
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| New! Test Tube Desorber Accessory for 5200 |
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The 5200 may use a desorption tube instead of the Pyroprobe filament rod for heating a sample. The desorption tube attaches pneumatically to the desorption probe, which brings flow through the tube and then to the trap of the 5200.
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The image below outlines the probe assembly. Click it to view a larger window, it will open in a new window.
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Flow goes through the test tube desorber from the top.
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CDS ANALYTICAL PYROPROBE PRODUCT COMPARISON
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Pyrolysis Feature Comparison
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5000
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5150
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5200
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PC Control of all features
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X
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X
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X
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pulsed pyrolysis and/ or 8 step temperature programmed pyrolysis per sample
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X
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X
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X
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Silcosteel interface
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X
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X
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X
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Easily removable transfer line to inlet of GC
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X
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X
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GC start for each step in the analysis
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X
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X
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X
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Reactant gas option
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X
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OPTIONAL Test tube desorber attachment
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X
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second heated zone for sorbent trap
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X
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Temperature programmable interface settable in 1C increments to 350C; programmble in 1C/min. increments to 60C/min.
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X
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X
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Manual isothermal interface mounted directly to injection port
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X
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pulse pyrolysis programmable in 1C increments to 1400C;
Heating rates: 0.01 -20.00C/ms
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X
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X
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X
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Programmed Pyrolysis heating rates: 0.01-999.9C/sec. and .01 to 999.9C/min.
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X
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X
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X
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OPTIONAL cryofocusing
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X
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X
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OPTIONAL Pyrolysis & Additives library
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X
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X
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X
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OPTIONAL High Pressure (0-500psi) Reactant Gas option
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X
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